Cyanogen Bromide → HCID 20509922, compound

HRID 1758240Notes

Reaction equation

HRID 1758240 reaction equation
CO[CH:3](OC)[CH2:4][NH:5][CH:6]([CH3:14])[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[NH2:13].[N:17]#[C:18]Br>>[CH3:14][CH:6]1[C:7]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[NH:13][C:18]2=[N:17][CH:3]=[CH:4][N:5]12

Participants

3

Reactant 2

HCID 10476Cyanogen BromideHCID 20509902HCID 20509902, compound

Product 1

HCID 20509922HCID 20509922, compound

Procedure

4 g of crude N-(2,2-dimethoxyethyl)-α-methyl-o-amino-benzylamine and 1.9 g cyanogen bromide are reacted and the product is worked up in the same manner as in Example 1e to afford the heading compound. M.p. 171°-172° (crystallisation from ethanol).

Workup

  1. customto afford the heading compound
  2. customM.p. 171°-172° (crystallisation from ethanol)

Sources & evidence

ORD record
ord-7c3a0996fe134ece957ce2f4f2a80129
Source dataset
uspto-grants-1983_02
Patent number
US04372956

Reaction notes

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