1,8-Octanediamine → HCID 178484957, compound

HRID 1758246Notes

Reaction equation

HRID 1758246 reaction equation
[C:1]([NH:9][C:10](=[N:13][CH3:14])SC)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[NH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][NH2:24]>>[C:1]([NH:9][C:10]([NH:13][CH3:14])=[N:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][NH2:24])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 242501,8-OctanediamineHCID 10688244N-benzoyl-N'-methyl-S-methylisothiourea

Product 1

HCID 178484957HCID 178484957, compound

Procedure

A mixture of N-benzoyl-N'-methyl-S-methylisothiourea and an excess of 1,8-diaminooctane is maintained at 60° for 5 hours to give a solid product which is washed with ether to leave N-benzoyl-N'-methyl-N"-(8-aminooctyl)guanidine.

Workup

  1. customto give a solid product which
  2. washis washed with ether

Sources & evidence

ORD record
ord-53826b3cd7684c60a98dadd192d4e202
Source dataset
uspto-grants-1983_02
Patent number
US04372963

Reaction notes

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