HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → 79444-77-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 6-Methylbenzofuran | HCID 86929 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | 79444-77-2 | HCID 20509979 | 80.8% |
Reaction Steps
A mixture of 6-methylbenzofuran (3.44 g, 0.026 mol), N-bromosuccinimide (4.63 g, 0.026 mol), dibenzoyl peroxide (trace) and carbon tetrachloride (50 cm3) was refluxed for 5 hr. The mixture was filtered and the solvent was removed from the filtrate. The residue was distilled to give 6-bromomethylbenzofuran (4.38 g, 0.021 mol, 80.0%) b.p. 84°-88° C./0.7 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04372970 |
| Source dataset | uspto-grants-1983_02 |
| ORD ID | ord-6650016259924ddf95994f70c80fc838 |
| Source note | uspto-grants-1983_02 |