HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → Ethyl 2-benzyloxyimino-3-oxobutyrate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178468382 | HCID 178468382 | — |
| Product | Ethyl 2-benzyloxyimino-3-oxobutyrate | HCID 53396355 | — |
Reaction Steps
A mixture of 2-hydroxyimino-3-oxobutyrate (syn isomer, 47.1 g.), benzylbromide (61.6 g.), potassium carbonate (62.2 g.), N,N-dimethylformamide (70 ml.) and ethyl acetate (70 ml.) was treated in a similar manner to that of Example A-(1) to give ethyl 2-benzyloxyimino-3-oxobutyrate (syn isomer, 70.0 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04372952 |
| Source dataset | uspto-grants-1983_02 |
| ORD ID | ord-da8350803e43462e82d53174669bd22a |
| Source note | uspto-grants-1983_02 |