HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → 2-[(1,1-Dioxidotetrahydro-3-thienyl)amino]ethanol hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | 3-Aminotetrahydrothiopene 1,1-dioxide hydrochloride | HCID 2795201 | — |
| Product | 2-[(1,1-Dioxidotetrahydro-3-thienyl)amino]ethanol hydrochloride | HCID 16896370 | — |
Reaction Steps
The procedure of Example 1 was repeated substituting 95 percent monoethanolamine (28.6 parts) for the ammonium hydroxide of Example 1. A sticky solid was filtered after treatment with hydrochloric acid, and upon drying in vacuo over P2O5 weighed 59.6 g. (78.5 percent of theory) m.p. 122°-124° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04374040 |
| Source dataset | uspto-grants-1983_02 |
| ORD ID | ord-86cb4db8a7b940b4a64ef7d396ff5961 |
| Source note | uspto-grants-1983_02 |