HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylmorpholine → HCID 13105135, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylmorpholine | HCID 7972 | — |
| Reactant | Isobutyl chloroformate | HCID 62365 | — |
| Reactant | L-Phenylalanine, N-[(1,1-dimethylethoxy)carbonyl]- | HCID 77857 | — |
| Reactant | HCID 13105133 | HCID 13105133 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 13105135 | HCID 13105135 | — |
Reaction Steps
The procedure of Example 1 is followed using 1 liter of ethylacetate, 30.68 ml of isobutyl chloroformate, 26.00 ml of N-methylmorpholine, 62.72 grams of BOC-phenylalanine and 68 grams of N-Me-Ala-Tyr-OMe affording 3 crops of product as follows:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04374060 |
| Source dataset | uspto-grants-1983_02 |
| ORD ID | ord-091ab446f2ca4fa2ac3de0fbeda120d8 |
| Source note | uspto-grants-1983_02 |