Maleic Acid → HCID 86738793, compound

HRID 1758478Notes

Reaction equation

HRID 1758478 reaction equation
[CH3:1][CH:2]1[CH2:19][CH2:18][C:5]2=[CH:6][CH:7]=[N:8][CH:9]=[CH:10][C:11]3[CH:17]=[CH:16][CH:15]=[CH:14][C:12]=3[O:13][CH:4]2[CH2:3]1.[C:20]([OH:27])(=[O:26])/[CH:21]=[CH:22]\[C:23]([OH:25])=[O:24]>C(O)C>[C:20]([OH:27])(=[O:26])/[CH:21]=[CH:22]\[C:23]([OH:25])=[O:24].[CH3:1][CH:2]1[CH2:19][CH2:18][C:5]2=[CH:6][CH:7]=[N:8][CH:9]=[CH:10][C:11]3[CH:17]=[CH:16][CH:15]=[CH:14][C:12]=3[O:13][CH:4]2[CH2:3]1

Participants

4

Reactant 2

HCID 444266Maleic AcidHCID 57353946HCID 57353946, compound

Product 1

HCID 86738793HCID 86738793, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent2×

Procedure

1.05 g 6,7,8,9-tetrahydro-7-methyl-5H-dibenz(b,i)(1,6)oxazecine was dissolved in 6 ml ethanol. A solution of 0.6 g maleic acid in 3 ml ethanol was added to this solution. The crystals formed were removed and subsequently washed with ether.

Workup

  1. customThe crystals formed
  2. customwere removed
  3. washsubsequently washed with ether

Sources & evidence

ORD record
ord-61124832982e4344ac8466a744afbd49
Source dataset
uspto-grants-1983_02
Patent number
US04374133

Reaction notes

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