HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 178433673, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 4-methoxy-N-[2-[(5-methyl-1H-imidazol-4-yl)methylsulfanyl]ethyl]-1,1-dioxo-1,2,5-thiadiazol-3-amine | HCID 178494335 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178433673 | HCID 178433673 | — |
Reaction Steps
When a methanolic solution of 3-{2-[(5-methyl-1H-imidazol-4-yl)methylthio]ethylamino}-4-methoxy-1,2,5-thiadiazole 1,1-dioxide [prepared by the procedure of Step A of Example 1] is treated with a solution of sodium hydroxide in methanol by the general procedure of Example 17, Step B, the title compound is produced, mp 263°-265° (dec).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04374248 |
| Source dataset | uspto-grants-1983_02 |
| ORD ID | ord-ee91714afa0642eab31c6617d32b6460 |
| Source note | uspto-grants-1983_02 |