5-(((2-Aminoethyl)thio)methyl)-N,N-dimethyl-2-furanmethanamine → HCID 178483228, compound

HRID 1758642Notes

Reaction equation

HRID 1758642 reaction equation
CO[C:3]1[C:7](OC)=[N:6][S:5](=[O:11])(=[O:10])[N:4]=1.[CH3:12][N:13]([CH2:15][C:16]1[O:20][C:19]([CH2:21][S:22][CH2:23][CH2:24][NH2:25])=[CH:18][CH:17]=1)[CH3:14].[Cl:26][C:27]1[C:28]([CH2:33][S:34][CH2:35][CH2:36][NH2:37])=[N:29][CH:30]=[CH:31][CH:32]=1>>[Cl:26][C:27]1[C:28]([CH2:33][S:34][CH2:35][CH2:36][NH:37][C:7]2[C:3]([NH:25][CH2:24][CH2:23][S:22][CH2:21][C:19]3[O:20][C:16]([CH2:15][N:13]([CH3:12])[CH3:14])=[CH:17][CH:18]=3)=[N:4][S:5](=[O:10])(=[O:11])[N:6]=2)=[N:29][CH:30]=[CH:31][CH:32]=1

Participants

4

Reactant 3

HCID 1622035-(((2-Aminoethyl)thio)methyl)-N,N-dimethyl-2-furanmethanamineHCID 122305383,4-Dimethoxy-1,2,5-thiadiazole 1,1-dioxideHCID 129515322-(3-Chloropyrid-2-ylmethylthio)ethylamine

Product 1

HCID 178483228HCID 178483228, compound

Procedure

When a methanolic solution of 3,4-dimethoxy-1,2,5-thiadiazole 1,1-dioxide is successively treated with 2-[(5-dimethylaminomethyl-2-furyl)methylthio]ethylamine and 2-[(3-chloro-2-pyridyl)methylthio]ethylamine, the title compound is thereby produced.

Sources & evidence

ORD record
ord-8a4a4515a8924f1fb9602c1d55ec50d5
Source dataset
uspto-grants-1983_02
Patent number
US04374248

Reaction notes

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