HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20508545, compound → [6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepin-8-yl]isocyanate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20508545 | HCID 20508545 | — |
| Reactant | HCID 20508551 | HCID 20508551 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | [6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepin-8-yl]isocyanate | HCID 20508564 | — |
Reaction Steps
A solution of [6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepin-8-yl]isocyanate is prepared as described in paragraph (a) of Example 1 from 7.0 g (22.6 mmol) of 8-amino-6-(o-chlorophenyl)-4H-s-triazolo-[4,3-a][1,4]benzodiazepine, but using methylene chloride in place of 1,2-dichloroethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04374773 |
| Source dataset | uspto-grants-1983_02 |
| ORD ID | ord-0a71b11faf4e4862a9b08d03de31a3f1 |
| Source note | uspto-grants-1983_02 |