HRID1758894

反应详情

EQUATION

反应方程式

HRID 1758894 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

This acid was prepared by refluxing 106.5 g (0.390 mol) of ethyl 5-(2',4'-dimethylphenyl)-5-cyano-4-ketopentanoate in 350 ml of glacial acetic acid, 122 ml of water, and 122 ml of concentrated sulfuric acid. The procedure is described in Example I, Part B. The product was obtained as a dark-colored viscous oil, 39.2 g (46% yield).

WORKUP

后处理

  1. customThis acid was prepared
  2. customThe product was obtained as a dark-colored viscous oil, 39.2 g (46% yield)