HRID1758990

反应详情

EQUATION

反应方程式

HRID 1758990 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 1-(4-benzyloxyphenyl) propan-2-one ethylene ketal (6 g) in ethanol (100 ml) was hydrogenated at 45 psi and ambient temperature in the presence of 10% Pd/C until hydrogen uptake had ceased. The solution was filtered and evaporated to give a light coloured oil which crystallised on standing m.p. 61°-64°.

WORKUP

后处理

  1. filtrationThe solution was filtered
  2. customevaporated
  3. customto give a light coloured oil which
  4. customcrystallised