Ethyl Thioglycolate → HCID 86738470, compound
Reaction equation
N(=[S:3]1[CH2:8][C:7](=[O:9])C=CN1)O.[NH2:10][C:11](C)(C)[CH:12]=[N:13][OH:14].ClCl.SCC(OCC)=O.[OH-].[Na+]>O>[N:13](=[C:12]1[CH2:11][NH:10][C:7](=[O:9])[CH2:8][S:3]1)[OH:14]Participants
7
Reactant 5
Product 1
Reagents, catalysts & solvents 1
Conditions
- Temperature
- 0 °C
Procedure
The oximino-thiazin-5-one compounds used as starting materials in preparing the compounds of this invention can be prepared by the methods disclosed in U.S. Pat. No. 4,071,627. In one method, a solution of α-aminoisobutyraldoxime and water is stirred and cooled to 0° C. Chlorine is added to the solution and the mixture is stirred. Ethyl mercaptoacetate and a base, such as sodium hydroxide, are added to produce an oximino-tetrahydro-1,4-thiazin-5-one.
Workup
- customin preparing the compounds of this invention
- customcan be prepared by the methods
Sources & evidence
- ORD record
- ord-1d776159f4184418bb7afe26a8204a57
- Source dataset
- uspto-grants-1982_07
- Patent number
- US04339444
Reaction notes
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