HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → Methyl acetylphosphonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | DIMETHYL ACETYLPHOSPHONATE | HCID 2785315 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Methyl acetylphosphonate | HCID 23674726 | — |
Reaction Steps
Dimethyl acetylphosphonate (10 g, 0.066 mol) and sodium iodide (15 g, 0.1 mol) were dissolved in acetone (80 ml) and the solution was stirred and refluxed for 6 hours. After cooling, the precipitated solid was filtered off, washed with acetone and ether and then air dried. Yield=9.5 g, m.p. decomp >170°. The NMR spectrum was consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04339443 |
| Source dataset | uspto-grants-1982_07 |
| ORD ID | ord-ab309c2de80d44e996ba08a004182480 |
| Source note | uspto-grants-1982_07 |