HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiosemicarbazide → HCID 178460685, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiosemicarbazide | HCID 2723789 | — |
| Reactant | HCID 178473688 | HCID 178473688 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178460685 | HCID 178460685 | — |
Reaction Steps
A mixture of sodium acetylmethylphosphinate (3.5 g) and thiosemicarbazide (2.2 g) was stirred in ethanol (15 ml) for 4 days. The precipitated hydrazone was filtered off and dried (4.6 g). The n.m.r spectrum supports the required structure. The compound slowly decomposes above 125°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04339443 |
| Source dataset | uspto-grants-1982_07 |
| ORD ID | ord-a1328fb88e744f3c8f301ee20ed05155 |
| Source note | uspto-grants-1982_07 |