HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 131712767, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4,5,6,7-Tetrahydro-4-oxothionaphthene | HCID 83418 | — |
| Product | HCID 131712767 | HCID 131712767 | — |
Reaction Steps
A mixture of 100 g. (0.60 mol) of the E-oxime of 4-oxo-4,5,6,7-tetrahydrobenzo[b]thiophene, 330 g. (3.6 mols) of epichlorohydrin and 391.2 g. (2.8 mols) of potassium carbonate in one liter of dimethylformamide is heated to 110° C. for 6 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04339450 |
| Source dataset | uspto-grants-1982_07 |
| ORD ID | ord-5e3eccaf6b7c4ee6be45b3de6939ffee |
| Source note | uspto-grants-1982_07 |