Methyl iodide → HCID 13938952, compound

HRID 1759354Notes

Reaction equation

HRID 1759354 reaction equation
[CH3:1][N:2]([CH3:10])[CH2:3][CH2:4][O:5][CH2:6][CH2:7][CH2:8][CH3:9].[CH3:11][I:12]>CCOCC>[I-:12].[CH3:1][N+:2]([CH3:11])([CH3:10])[CH2:3][CH2:4][O:5][CH2:6][CH2:7][CH2:8][CH3:9]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 5469642-Butoxy-N,N-dimethylethanamine

Product 1

HCID 13938952HCID 13938952, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

10 g dimethyl(2-butoxyethyl)amine and 10 g methyl iodide were stirred in 125 ml ether for 24 hours. The precipitate was filtered off and dried. The trimethyl(2-butoxyethyl)ammonium iodide obtained had a melting point of 71°-73° C.

Workup

  1. filtrationThe precipitate was filtered off
  2. customdried

Sources & evidence

ORD record
ord-fcaf2ac2857f4bdf8d0b4ed7bfbdea68
Source dataset
uspto-grants-1982_07
Patent number
US04340698

Reaction notes

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