3-Bromo-1,1-diphenylacetone → HCID 15571315, compound

HRID 1759376Notes

Reaction equation

HRID 1759376 reaction equation
[Br:1][CH2:2][C:3](=[O:17])[CH:4]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)[C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1.[NH:18]1[CH2:25][CH2:24][CH2:23][CH2:22][CH2:21][NH:20][C:19]1=[S:26]>>[BrH:1].[C:5]1([CH:4]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[C:3]2([OH:17])[N:20]3[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][N:18]=[C:19]3[S:26][CH2:2]2)[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1

Participants

3

Reactant 2

HCID 27946353-Bromo-1,1-diphenylacetoneHCID 53727341,3-Diazocane-2-thione

Product 1

HCID 15571315HCID 15571315, compound

Procedure

1-Bromo-3,3-diphenyl-2-propanone is reacted with hexahydro-1,3-diazocin-2(1H)-thione by the procedure of Example 22, giving the desired product, m.p. 211°-213° C. (dec.).

Sources & evidence

ORD record
ord-121a7eb94e594ce7baa9f41f3c96f699
Source dataset
uspto-grants-1982_07
Patent number
US04340734

Reaction notes

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