1-Nitro-4-tert-butyl-2,6-dimethylbenzene → 4-Tert-butyl-2,6-dimethylaniline

HRID 1759454Notes

Reaction equation

HRID 1759454 reaction equation
[N+:1]([C:4]1[C:9]([CH3:10])=[CH:8][C:7]([C:11]([CH3:14])([CH3:13])[CH3:12])=[CH:6][C:5]=1[CH3:15])([O-])=O.[H][H]>>[CH3:15][C:5]1[CH:6]=[C:7]([C:11]([CH3:13])([CH3:12])[CH3:14])[CH:8]=[C:9]([CH3:10])[C:4]=1[NH2:1]

Participants

3

Reactant 2

HCID 2233901-Nitro-4-tert-butyl-2,6-dimethylbenzeneHCID 178418361HCID 178418361, compound

Product 1

HCID 12296974-Tert-butyl-2,6-dimethylaniline

Procedure

contacting the 2-nitro-1,3-dimethyl-5-tertiarybutylbenzene with hydrogen in the presence of a hydrogenation catalyst at a temperature of from about 0° C. to about 200° C. and a pressure of from about 0 psig to about 2000 psig to form 2,6-dimethyl-4-tertiary-butylaniline;

Workup

  1. customof from about 0° C. to about 200° C.

Sources & evidence

ORD record
ord-9c897d71ff1b4763bdaac51772a0bea9
Source dataset
uspto-grants-1982_07
Patent number
US04340758

Reaction notes

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