Thionyl Chloride → HCID 20531325, compound

HRID 1759588Notes

Reaction equation

HRID 1759588 reaction equation
[CH3:1][C:2]1([CH3:20])[C:10]2[C:5](=[CH:6][C:7]([O:11][CH:12]([CH2:16][CH3:17])[C:13](O)=[O:14])=[CH:8][CH:9]=2)[C:4]([CH3:19])([CH3:18])[CH2:3]1.S(Cl)([Cl:23])=O>>[CH3:1][C:2]1([CH3:20])[C:10]2[C:5](=[CH:6][C:7]([O:11][CH:12]([CH2:16][CH3:17])[C:13]([Cl:23])=[O:14])=[CH:8][CH:9]=2)[C:4]([CH3:19])([CH3:18])[CH2:3]1

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 20531320HCID 20531320, compound

Product 1

HCID 20531325HCID 20531325, compound

Procedure

A mixture of 100.5 g (0.364 mole) of 2-(1,1,3,3-tetramethyl-5-indanoxy)-butyric acid and 67 ml of thionyl chloride were refluxed for 2 hours. The excess thionyl chloride was evaporated.

Workup

  1. temperaturewere refluxed for 2 hours
  2. customThe excess thionyl chloride was evaporated

Sources & evidence

ORD record
ord-725a5fa85a694259b57abc81a60ce81b
Source dataset
uspto-grants-1982_07
Patent number
US04341864

Reaction notes

Loading…