HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzaldehyde → HCID 22600056, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzaldehyde | HCID 68023 | — |
| Reactant | 4-(Methylsulfinyl)aniline | HCID 11435065 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 22600056 | HCID 22600056 | — |
Reaction Steps
A mixture of 3.0 g (19 mmol) of 4-methylsulfinylaniline (obtained in reference example 3), 2 mL (19 mmol) of 4-fluorobenzaldehyde and 80 mL of benzene was refluxed in a Dean-Stark for 2 days. The solvent was removed and the crude product obtained was directly used in the next reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06838476B1 |
| Source dataset | uspto-grants-2005_01 |
| ORD ID | ord-4f6bba6e08f140aaba54235952f89967 |
| Source note | uspto-grants-2005_01 |