HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dichlorobenzoic acid → 3,5-Dichlorobenzylic alcohol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dichlorobenzoic acid | HCID 5811 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Product | 3,5-Dichlorobenzylic alcohol | HCID 43236 | 74.1% |
Reaction Steps
Prepared according to the method described in Example X(i) above from 3,5-dichlorobenzoic acid (15.3 g; 80 mmol), TEA (8.9 g; 88 mmol), i-Bu chloroformate (12 g; 88 mmol) and NaBH4 (9.0 g; 240 mmol), yielding 10.5 g (74%) of sub-title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06838478B2 |
| Source dataset | uspto-grants-2005_01 |
| ORD ID | ord-9b772853db5943ba80cde82dc6eb6237 |
| Source note | uspto-grants-2005_01 |