Benzoyl chloride → HCID 178489091, compound

HRID 1760174Notes

Reaction equation

HRID 1760174 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[NH:13][N:12]=[C:11]([CH3:14])[C:10]=2[NH2:15])=[CH:5][CH:4]=1.[C:16](Cl)(=[O:23])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([C:9]2[NH:13][N:12]=[C:11]([CH3:14])[C:10]=2[NH:15][C:16](=[O:23])[C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)=[CH:7][CH:8]=1

Participants

3

Reactant 2

HCID 7412Benzoyl chlorideHCID 178489089HCID 178489089, compound

Product 1

HCID 178489091HCID 178489091, compound

Procedure

The preparation took place in analogy with Example 15a), starting with 500 mg of 5-(4-methoxyphenyl)-3-methyl-1H-pyrazol-4-ylamine (50) and 315 μl of benzoyl chloride. The following was obtained: 51 C18H17N3O2 (307.36) MS (ESI) 308 (M+H)

Workup

  1. customThe following was obtained

Sources & evidence

ORD record
ord-9121f1fe79ae478dbcea6968eaab5238
Source dataset
uspto-grants-2005_01
Patent number
US06841556B2

Reaction notes

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