HRID1760538

反应详情

EQUATION

反应方程式

HRID 1760538 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
130 °C

PROCEDURE

实验过程

A mixture of 267 mg of 4-chloro-2-(4-chlorophenyl)-6-isopropylpyrimidine and 522 mg of morpholine was heated at 130° C. for 2 hours. After cooling, 20 ml of water were added, the mixture was stirred, and the solid was filtered off with suction and dried at 50° C. in vacuo. Yield: 0.28 g.

WORKUP

后处理

  1. temperatureAfter cooling
  2. filtrationthe solid was filtered off with suction
  3. customdried at 50° C. in vacuo