HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Acetyl-5-bromo-4-chloro-1H-indol-3-yl acetate → HCID 9964843, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Acetyl-5-bromo-4-chloro-1H-indol-3-yl acetate | HCID 76416 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 9964843 | HCID 9964843 | — |
Reaction Steps
To a stirred solution of 5-bromo-4-chloroindoxyl 1,3-diacetate (25) (1.0 g, 3.03 mmol) in anhydrous N,N-dimethylformamide (3 mL) was added sodium methoxide (270 mg, 5.00 mmol). The resulting dark-colored reaction mixture was degassed with nitrogen (g) for 30 min at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06844346B2 |
| Source dataset | uspto-grants-2005_01 |
| ORD ID | ord-edaa05a10a1d447da0f0c2dda099df05 |
| Source note | uspto-grants-2005_01 |