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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1760539Generated: October 30, 2026

1-Acetyl-5-bromo-4-chloro-1H-indol-3-yl acetate → HCID 9964843, compound

https://huagongshe.com/reaction/1760539

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Acetyl-5-bromo-4-chloro-1H-indol-3-yl acetateHCID 76416—
ReactantSodium MethoxideHCID 10942334—
SolventDimethylformamideHCID 6228—
ProductHCID 9964843HCID 9964843—

Reaction Steps

To a stirred solution of 5-bromo-4-chloroindoxyl 1,3-diacetate (25) (1.0 g, 3.03 mmol) in anhydrous N,N-dimethylformamide (3 mL) was added sodium methoxide (270 mg, 5.00 mmol). The resulting dark-colored reaction mixture was degassed with nitrogen (g) for 30 min at room temperature.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06844346B2
Source datasetuspto-grants-2005_01
ORD IDord-edaa05a10a1d447da0f0c2dda099df05
Source noteuspto-grants-2005_01