HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1760675Generated: October 29, 2026
Dimethyl Sulfoxide → HCID 69779737, compound
https://huagongshe.com/reaction/1760675
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethyl Sulfoxide | HCID 679 | — |
| Reactant | 3-Pentanamine | HCID 12019 | — |
| Reactant | 2-(4-Chloro-2,6-dimethyl-phenoxy)-4-chloro-6-methyl-nicotinic acid methyl ester | HCID 24806260 | — |
| Product | HCID 69779737 | HCID 69779737 | — |
Reaction Steps
A mixture of 4-chloro-6-methyl-2-(4-Chloro-2,6-dimethyl-phenoxy)-nicotinic acid methyl ester (77 mg, 0.226 mmol) and 1-ethyl-propyl-amine in DMSO was heated at 120° C. for 4 hr. The mixture was quenched with sat. ammonium chloride, water, brine and extracted with ethyl acetate. The organic layer was dried and concentrated to give 140 mg of yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06844351B1 |
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| Source dataset | uspto-grants-2005_01 |
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| ORD ID | ord-b19e2b86138541f296cbbbc5ce29d8b0 |
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| Source note | uspto-grants-2005_01 |
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