HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 22593947, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 9930450 | HCID 9930450 | — |
| Product | HCID 22593947 | HCID 22593947 | 74% |
Reaction Steps
The title compound (0.23 g, 74%) was prepared as a white solid from 3-[4-[2-(2,3-dihydro-1,4-benzoxazin-4-yl)ethoxy]phenyl]-2-ethoxypropanoic acid (0.3 g, 0.8 mmol) obtained in example 26 and methylamine (40% solution) ( 2 mL) by an analogous procedure to that described in example 32.mp: 97-99° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06846824B2 |
| Source dataset | uspto-grants-2005_01 |
| ORD ID | ord-73fa59cfe9da4a0fa5d57edd780326f4 |
| Source note | uspto-grants-2005_01 |