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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1761244Generated: November 1, 2026

Imidazole → HCID 129689385, compound

https://huagongshe.com/reaction/1761244

Reaction equation

Participants

RoleNameHCIDCharge
ReactantImidazoleHCID 795—
ReactantTetrafluoroboric acidHCID 28118—
SolventDiethyl EtherHCID 3283—
SolventDichloromethaneHCID 6344—
ProductHCID 129689385HCID 129689385—

Reaction Steps

To a solution of imidazole (20 mmol) in dichloromethane (30 mL) at 0° C. HBF4 (20 mmol, 3.8 g of a diethyl etherate) in dichloromethane is added dropwise. The reaction mixture is diluted with diethyl ether (100 mL) to precipitate the title compound. It is then filtered, washed with ether and recrystallized from ether.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06846922B1
Source datasetuspto-grants-2005_01
ORD IDord-d1a4b8e39ec0483ca18d877a565441c4
Source noteuspto-grants-2005_01