HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 19833632, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 2-Chloromethyl-4-methoxy-pyridine | HCID 10487136 | — |
| Reactant | 2-Chloro-6-(chloromethyl)pyridine | HCID 15574440 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19833632 | HCID 19833632 | — |
Reaction Steps
The hydroxymethyl compound obtained above was converted to 2-chloromethyl-4-methoxypyridine by the method of Part (iv), above, to provide 0.895 g (5.68 mmole). This was reacted with an equimolar amount of triphenylphosphine in toluene (10 ml) at reflux for 20 hours. The precipitated product was filtered to give 860 mg of the title compound as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04826833 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-bdfde632030b4d24b84658e35b48cfed |
| Source note | uspto-grants-1989_05 |