HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → ST025572
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-Methoxybenzoic acid | HCID 11370 | — |
| Reactant | N-Hydroxysuccinimide | HCID 80170 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | ST025572 | HCID 716774 | 89.7% |
Reaction Steps
O-anisic acid (1.0 g), N-hydroxysuccinimide (0.76 g) and water-soluble carbodiimide hydrochloride (1.39 g) were dissolved in methylene chloride (15 ml), and the solution was stirred overnight at room temperature. The precipitate was removed by filtration. The mother liquor was concentrated under reduced pressure, and the residue was crystallized from isopropanol to give 1.47 g of N-(2-methoxybenzoyloxy)succinimide (mp. 180°-182° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04826814 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-184b570e39cc450aabcdaaebe8ba4a44 |
| Source note | uspto-grants-1989_05 |