HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl formate → N-[3-(Trimethoxysilyl)propyl]formamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl formate | HCID 7865 | — |
| Reactant | Aminopropyltrimethoxysilane | HCID 83756 | — |
| Product | N-[3-(Trimethoxysilyl)propyl]formamide | HCID 14388644 | — |
Reaction Steps
A mixture of 7 parts (39 mmol.) of 3-aminopropyltrimethoxysilane and 20 parts (330 mmol.) of methyl formate was heated under reflux in a nitrogen atmosphere. The reaction was monitored by gas chromatography and was found to be complete after 3 hours. Volatiles were then removed in vacuum, yielding the desired N-(3-trimethoxysilylpropyl)formamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04826915 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-4afe7c874db2458d92fb75bdedf29fdc |
| Source note | uspto-grants-1989_05 |