Alumina → HCID 131715939, compound

HRID 1761790Notes

Reaction equation

HRID 1761790 reaction equation
[OH2:1].O.O.[N+:4]([O-:7])([O-:6])=[O:5].[Pd+2:8].[N+]([O-])([O-])=[O:10].[O-2].[O-2].[O-2].[Al+3:16].[Al+3]>O>[Pd:8].[N+:4]([O-:7])([O-:6])=[O:5].[O-2:10].[O-2:1].[O-2:5].[Al+3:16].[Al+3:16]

Participants

4

Reactant 2

HCID 9989226AluminaHCID 131715940HCID 131715940, compound

Product 1

HCID 131715939HCID 131715939, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Palladium (II) nitrate trihydrate (0.270 g) was dissolved in water (21.0 ml) and added to gamma-alumina (5.0 g, from calcination of Catapal SB boehmite alumina in air at 580° C.) with stirring. Water was slowly removed in vacuo keeping the catalyst temperature about 55° C. and the catalyst was then dried further at 100° C. for 12 hours.

Workup

  1. customWater was slowly removed in vacuo
  2. customthe catalyst temperature about 55° C.
  3. customthe catalyst was then dried further at 100° C. for 12 hours

Sources & evidence

ORD record
ord-523d0db1405a4bf8bdefe683ebbf0b52
Source dataset
uspto-grants-1989_05
Patent number
US04827070

Reaction notes

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