HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,5-Dihydroacephenanthrylene-6-carbaldehyde → 6-Acephenanthrylenecarbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,5-Dihydroacephenanthrylene-6-carbaldehyde | HCID 14459539 | — |
| Solvent | Toluene hexane | HCID 21889329 | — |
| Product | 6-Acephenanthrylenecarbaldehyde | HCID 14371439 | 35.8% |
Reaction Steps
Using the dehydrogenation procedure outlined in Example 7B, 4,5-dihydroacephenanthrylene-6-carbaldehyde (J. P. Hoeffinger, P. Jacquignon, and N. P. Buu-Hoi, Bull. Soc. Chim. Fr. 974 (1970)) gave a 35.8% yield of 6-acephenanthrylenecarbaldehyde, mp 161°-163° (dec), (C, H), (PhCH3 /hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04827034 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-497df8ee3b9a44b3b027a3601ec21f0c |
| Source note | uspto-grants-1989_05 |