HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 20043561, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Tert-Butylamine | HCID 6385 | — |
| Reactant | 5-Ethenyl-2-hydroxybenzaldehyde | HCID 20043562 | — |
| Product | HCID 20043561 | HCID 20043561 | 79% |
Reaction Steps
73 g (1 mole) of tert-butylamine were added to a solution of 74 g (0.5 mole) of 2-hydroxy-5-vinylbenzaldehyde in 750 ml of toluene, and this mixture was refluxed for 2 hours. After extraction with twice 500 ml of ice water, the toluene was distilled off. 80 g (79%) of 2-butylaminomethyl-4-vinylphenol were obtained as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04828941 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-1925280729ab4d3ebbde2655ba25011d |
| Source note | uspto-grants-1989_05 |