Sodium borohydride → HCID 14125980, compound

Participants

Reaction Steps

1.2 g of sodium borohydride were added to a solution of 13.8 g (0.06 mol) of 4-fluorophenyl 1-(1, 2, 4-triazol-1-yl)-cyclopropyl ketone in 50 ml of methanol, the mixture was refluxed for 1 hour, and 12.4 g (89%) of the title compound, melting point 104°-106° C., were isolated by working up using dichloromethane/water.

Provenance & Evidence