HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → HCID 22411936, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | HCID 15067843 | HCID 15067843 | — |
| Solvent | Thionyl Chloride | HCID 24386 | — |
| Product | HCID 22411936 | HCID 22411936 | — |
Reaction Steps
27 g of 2-phenyl-4-(1-hydroxy-2-methylpropyl)-5-methyl-1H-imidazole are dissolved in 700 ml of chloroform with 44 ml of SOCl2 and refluxed for 5 hours. 2-Phenyl-5-methyl-4-(1-chloro-2-methylpropyl)-1H-imidazole hydrochloride is isolated in quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04829065 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-aa909402dd8548279fc05fdc5ca16f33 |
| Source note | uspto-grants-1989_05 |