HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetraethylene Glycol → HCID 86743028, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetraethylene Glycol | HCID 8200 | — |
| Reactant | Benzoyl chloride, 3-nitro- | HCID 8495 | — |
| Product | HCID 86743028 | HCID 86743028 | — |
Reaction Steps
Tetraethylene glycol (58.2 g, 0.3 mole) was treated with m-nitrobenzoyl chloride, following the general procedure described in Example 1, Part A. After the usual work-up, the product was crystallized from ethyl acetate/hexanes at -20° C. for 3 days to give bis-(3-nitrobenzoyl)-tetraethylene glycol (110 g) as a pale yellow solid, m.p. 38°-40° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04829099 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-01e73624ce84441b9ddde6db9e0d2a3a |
| Source note | uspto-grants-1989_05 |