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HRID1761985

反应详情

EQUATION

反应方程式

HRID 1761985 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)c1ccc([N+](=O)[O-])cc1
HCID8502

4-Nitrobenzoyl chloride

C7H4ClNO3

结构：CC(O)COC(C)COC(C)CO
HCID32611

2-[2-(2-Hydroxypropoxy)propoxy]propan-1-ol

C9H20O4

PRODUCTS

生成物

1
结构：CC(CO)OCC(C)OCC(O)C(C(=O)c1ccc([N+](=O)[O-])cc1)C(=O)c1ccc([N+](=O)[O-])cc1
HCID86743032

未命名化合物

收率 89%

PROCEDURE

实验过程

Tripropylene glycol (57.6 g, 0.3 mole) was treated with p-nitrobenzoyl chloride (116 g, 0.625 mole), following the general procedure described in Example 1, Part A. The product, bis-(4-nitrobenzoyl)-tripropylene glycol (131 g), was obtained as a viscous yellow oil.