HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Hydroxide → Sodium 4-[2-(4-isopropylbenzamido)ethoxy]benzoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | 4-(2-(4-Isopropylbenzamido)ethoxy)benzoic acid | HCID 3081027 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | Sodium 4-[2-(4-isopropylbenzamido)ethoxy]benzoate | HCID 23698334 | 70,5% |
Reaktionsschritte
4-[2-(4-Isopropylbenzamido)ethoxy]benzoic acid (3.27 g) was dissolved in 50 ml of methanol, a solution of 0.40 g of sodium hydroxide in 5 ml of water was added thereto, the mixture was concentrated in vacuo, and crystallized residue was recrystallised from methanol to give 2.46 g of crystalline product, m.p. not lower than 300° C. IR γmaxKBr (cm-1): 1640, 1605.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04831055 |
| Quelldatensatz | uspto-grants-1989_05 |
| ORD ID | ord-7b32c7d60e314b2d994c5846a8455aac |
| Quellennotiz | uspto-grants-1989_05 |