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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1762177Erstellt: 26. Oktober 2026

Sodium Hydroxide → Sodium 4-[2-(4-isopropylbenzamido)ethoxy]benzoate

https://huagongshe.com/reaction/1762177

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktSodium HydroxideHCID 14798—
Edukt4-(2-(4-Isopropylbenzamido)ethoxy)benzoic acidHCID 3081027—
LösungsmittelMethanolHCID 887—
LösungsmittelWaterHCID 962—
ProduktSodium 4-[2-(4-isopropylbenzamido)ethoxy]benzoateHCID 2369833470,5%

Reaktionsschritte

4-[2-(4-Isopropylbenzamido)ethoxy]benzoic acid (3.27 g) was dissolved in 50 ml of methanol, a solution of 0.40 g of sodium hydroxide in 5 ml of water was added thereto, the mixture was concentrated in vacuo, and crystallized residue was recrystallised from methanol to give 2.46 g of crystalline product, m.p. not lower than 300° C. IR γmaxKBr (cm-1): 1640, 1605.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04831055
Quelldatensatzuspto-grants-1989_05
ORD IDord-7b32c7d60e314b2d994c5846a8455aac
Quellennotizuspto-grants-1989_05