Sodium Hydroxide → HCID 20042507, compound

HRID 1762192Notes

Reaction equation

HRID 1762192 reaction equation
[NH2:1][C:2]1[C:7]([O:8][CH:9]([NH:17][C:18](=[O:24])[CH2:19][O:20]C(=O)C)[C:10]2[C:15]([CH3:16])=[CH:14][CH:13]=[CH:12][CH:11]=2)=[CH:6][CH:5]=[CH:4][N:3]=1.[OH-].[Na+]>CO>[NH2:1][C:2]1[C:7]([O:8][CH:9]([NH:17][C:18](=[O:24])[CH2:19][OH:20])[C:10]2[C:15]([CH3:16])=[CH:14][CH:13]=[CH:12][CH:11]=2)=[CH:6][CH:5]=[CH:4][N:3]=1

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 20042534HCID 20042534, compound

Product 1

HCID 20042507HCID 20042507, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

A solution of 2-amino-3-(2-acetoxyacetamido-6-methylbenzyloxy)pyridine (0.63 g) and 1N sodium hydroxide solution (2 ml) in methanol (20 ml) was stirred at room temperature for 1 hour. The resulting precipitates were collected by filtration to give 2-amino-3-(2-hydroxyacetamido-6-methylbenzyloxy)pyridine.

Workup

  1. customThe resulting precipitates
  2. filtrationwere collected by filtration

Sources & evidence

ORD record
ord-22199690b83349dc8153447136c22c03
Source dataset
uspto-grants-1989_05
Patent number
US04831041

Reaction notes

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