HRID1762198
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A solution of potassium cyanate (1.62 g) in water (5 ml) was dded dropwise to a mixture of 2-amino-6-methylbenzyl alcohol (1.37 g), water (5 ml), and acetic acid (6 ml) at room temperature. After being stirred for 2.5 hours, the resulting precipitates were collected by filtration, washed with water, and dried to give 6-methyl-2-ureidobenzyl alcohol (1.33 g).
WORKUP
后处理
- customthe resulting precipitates
- filtrationwere collected by filtration
- washwashed with water
- customdried