HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 14368441, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 20042521 | HCID 20042521 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 14368441 | HCID 14368441 | 62.2% |
Reaction Steps
A solution of 3-(2-acetoxymethylbenzyloxy)-2nitropyridine (7.8 g) in methanol (39 ml) and 1N aqueous sodium hydroxide (23 ml) was stirred at room temperature for 0.5 hours. To the mixture was added water (50 ml) and the precipitates were collected by filtration to give 3-(2-hydroxymethylbenzyloxy)-2-nitropyridine (4.18 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04831041 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-bc743177ac2b4ff1b48d5823d7271cd5 |
| Source note | uspto-grants-1989_05 |