HCID 841313, compound → HCID 67932470, compound

HRID 1762341Notes

Reaction equation

HRID 1762341 reaction equation
NC1C=CC(C2C=C(C)C=CC=2S(C2C=CC(C)=CC=2C2C=CC(N)=C([N+]([O-])=O)C=2)=O)=CC=1[N+]([O-])=O.[C:37]1([S:43]([C:45]2[CH:50]=[CH:49][C:48]([Cl:51])=[C:47]([N+:52]([O-])=O)[CH:46]=2)=[O:44])[CH:42]=[CH:41][CH:40]=[CH:39][CH:38]=1>>[C:37]1([S:43]([C:45]2[CH:50]=[CH:49][C:48]([Cl:51])=[C:47]([NH2:52])[CH:46]=2)=[O:44])[CH:42]=[CH:41][CH:40]=[CH:39][CH:38]=1

Participants

3

Reactant 2

HCID 841313HCID 841313, compoundHCID 53642139(4-Amino-3-nitrophenyl)-4-methylphenyl sulfoxide

Product 1

HCID 67932470HCID 67932470, compoundYield 90%

Procedure

Following the procedure described in Example 40 but using as a starting material instead of (4-amino-3-nitrophenyl)-4-methylphenyl sulfoxide a corresponding amount of phenyl-(4-chloro-3-nitrophenyl) sulfoxide, the title compound is obtained.

Sources & evidence

ORD record
ord-120a826b3ffc4c1da75d1558851aea79
Source dataset
uspto-grants-1989_05
Patent number
US04831194

Reaction notes

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