HCID 20075263, compound → HCID 20075278, compound

HRID 1762345Notes

Reaction equation

HRID 1762345 reaction equation
NC1C=CC(C2C=C(C)C=CC=2S(C2C=CC(C)=CC=2C2C=CC(N)=C([N+]([O-])=O)C=2)=O)=CC=1[N+]([O-])=O.[CH3:37][O:38][C:39]1[CH:44]=[CH:43][C:42]([S:45]([C:47]2[CH:52]=[CH:51][CH:50]=[CH:49][CH:48]=2)=[O:46])=[CH:41][C:40]=1[N+:53]([O-])=O>>[NH2:53][C:40]1[CH:41]=[C:42]([S:45]([C:47]2[CH:48]=[CH:49][CH:50]=[CH:51][CH:52]=2)=[O:46])[CH:43]=[CH:44][C:39]=1[O:38][CH3:37]

Participants

3

Reactant 2

HCID 20075263HCID 20075263, compoundHCID 53642139(4-Amino-3-nitrophenyl)-4-methylphenyl sulfoxide

Product 1

HCID 20075278HCID 20075278, compoundYield 89%

Procedure

Following the procedure described in Example 40 but using as a starting material instead of (4-amino-3-nitrophenyl)-4-methylphenyl sulfoxide a corresponding amount of (4-methoxy-3-nitrophenyl)-phenyl sulfoxide, the title compound is obtained.

Sources & evidence

ORD record
ord-617b1bb15d2e42d883820909ccdb625e
Source dataset
uspto-grants-1989_05
Patent number
US04831194

Reaction notes

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