Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Bicarbonate → 1-[[p-(Dimethylamino)benzylidene]amino]-2-ethylimidazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Bicarbonate | HCID 516892 | — |
| 반응물 | 1-[[p-(Dimethylamino)benzylidene]amino]-2-ethylimidazole hydrochloride | HCID 70351905 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 1-[[p-(Dimethylamino)benzylidene]amino]-2-ethylimidazole | HCID 54550057 | — |
반응 단계
The base is liberated from 7.3 g (26 mmol) of 1-[[p-(dimethylamino)benzylidene]amino]-2-ethylimidazole hydrochloride with saturated sodium hydrogen carbonate solution. This base is taken up in methylene chloride. The solution is dried over sodium sulphate and concentrated. There is obtained 1-[[p-(dimethylamino)benzylidene]amino]-2-ethylimidazole of melting point 120°-121°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04831151 |
| 출처 데이터셋 | uspto-grants-1989_05 |
| ORD ID | ord-aacee26615a742b382ca9bd36264c801 |
| 출처 메모 | uspto-grants-1989_05 |