HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Dimethylamino)Benzaldehyde → HCID 70351686, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Dimethylamino)Benzaldehyde | HCID 7479 | — |
| Reactant | HCID 17994043 | HCID 17994043 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 70351686 | HCID 70351686 | — |
Reaction Steps
1.49 g (10 mmol) of 4-dimethylamino-benzaldehyde are added to a solution of 0.88 g (5 mmol) of 1,3-diamino-2-propyl-imidazolium chloride in 15 ml of glacial acetic acid. After leaving to stand at room temperature for 2 days the product is crystallized out by the addition of ether and then recrystallized from ethanol. There is obtained 1,3-bis[[p-(dimethylamino)benzylidene]amino]-2-propyl-imidazolium chloride of melting point 252°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04831151 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-1f0ea12ac166457ba913c51d8a6a992b |
| Source note | uspto-grants-1989_05 |