HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-4-(chloromethyl)benzene → HCID 178437568, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-4-(chloromethyl)benzene | HCID 7723 | — |
| Reactant | 1-Benzylideneamino-2-ethylimidazole | HCID 54091172 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178437568 | HCID 178437568 | — |
Reaction Steps
1.61 g (10 mmol) of p-chlorobenzyl chloride are added to a solution of 1.99 g (10 mmol) of 1-(benzylidene)amino-2-ethylimidazole in 10 ml of acetonitrile. After heating under reflux for 24 hours the precipitated product is filtered off and recrystallized from ethanol/ether. There is obtained 1-(benzylideneamino)-3-(p-chlorobenzyl)-2-ethylimidazolium chloride of melting point >200°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04831151 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-35b14f43cb564496b124397b9c68b316 |
| Source note | uspto-grants-1989_05 |