HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 178437569, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178437568 | HCID 178437568 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178437569 | HCID 178437569 | — |
Reaction Steps
500 mg (1.39 mmol) of 1-(benzylideneamino)-3-(p-chlorobenzyl)-2-ethylimidazolium chloride are subjected to a steam distillation in 5 ml of water and 2 ml of 3N hydrochloric acid until benzaldehyde no longer evolves. The mixture is evaporated and the residue is recrystallized from ethanol/ether. There is obtained 1-amino-3-(p-chlorobenzyl)-2-ethylimidazolium chloride of melting point 223°-225°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04831151 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-0bc8a9fecae446ac9ab5f2b32643baf6 |
| Source note | uspto-grants-1989_05 |