HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Chlorophenacyl bromide → HCID 178437684, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Chlorophenacyl bromide | HCID 68303 | — |
| Reactant | 1-Benzylideneamino-2-ethylimidazole | HCID 54091172 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 178437684 | HCID 178437684 | — |
Reaction Steps
2.33 g (10 mmol) of p-chlorophenacyl bromide are added to a solution of 1.99 g (10 mmol) of 1-(benzylidene)amino-2-ethylimidazole in 30 ml of ethylene chloride. After stirring at 60° for 2 hours the product is filtered off and washed with ether. There is obtained 1-(benzylideneamino)-3-(p-chlorophenacyl)-2-ethylimidazolium bromide of melting point 236°-237°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04831151 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-ffb1476408d146adb726c07fbd6dbc15 |
| Source note | uspto-grants-1989_05 |