HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloride → HCID 13747682, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloride | HCID 312 | — |
| Reactant | 3-Methyl-1-propyl-3,9-dihydro-1H-purine-2,6-dione | HCID 174907 | — |
| Reactant | 3-Methyl-7-(5-oxohexyl)-1-propyl-3,7-dihydro-1H-purine-2,6-dione | HCID 12902748 | — |
| Reactant | 1-Chloro-5-hydroxy-5-methylhexane | HCID 13747679 | — |
| Reactant | HCID 178418573 | HCID 178418573 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 13747682 | HCID 13747682 | — |
Reaction Steps
Both alkylation of 3-methyl-1-propylxanthine with 1-chloro-5-hydroxy-5-methylhexane analogously to the following example 4 and Grignard synthesis with 3-methyl-7-(5-oxohexyl)-1-propylxanthine and methylmagnesium bromide or chloride in anhydrous tetrahydrofuran led to the same compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04833146 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-d383bd78c62042fc9002027184b66f1e |
| Source note | uspto-grants-1989_05 |